采用水热法制备了一系列纳米硅铝酸盐材料,考察了晶化时间、模板剂、硅源、铝源、稀土离子掺杂等对材料制备的影响.发现以TEAOH为模板剂,白炭黑为硅源,硫酸铝为铝源,铈离子掺杂制备的硅铝酸盐在苯甲醛与吲哚的Friedel-Crafts烷基化反应中的催化活性最好.通过XRD,BET和SEM表征了该材料的结构特性.
[1] 刘蕾, 马天翼, 袁忠勇, Liu Lei, Ma Tianyi, Yuan Zhongyong. 分级结构介孔-大孔材料及其实际应用 [J]. 石油化工 2011.
[2] 严子春, 胡家炜, Yan Zichun, Hu Jiawei. 新型多功能净水滤料的制备及其性能研究 [J]. 水处理技术 2009.
[3] 沈志虹, 师为, 李红杰, SHEN Zhi-hong, SHI Wei, LI Hong-jie. Cr改性USY分子筛提高裂化催化剂的异构化性能 [J]. 燃料化学学报 2005.doi:10.3969/j.issn.0253-2409.2005.03.022
[4] 丁士文, 张红军, 张永芬, 张圆圆, DING Shi-wen, ZHANG Hong-jun, ZHANG Yong-fen, ZHANG Yuan-yuan. 混晶纳米二氧化钛乳液光催化降解农药的研究 [J]. 河北大学学报（自然科学版） 2010.doi:10.3969/j.issn.1000-1565.2010.01.011
[5] 许迪欧, 王润伟, 付伟伟, 王影, 张宗弢, 裘式纶, XU Di-Ou, WANG Run-Wei, FU Wei-Wei, WANG Ying, ZHANG Zong-Tao, QIU Shi-Lun. 层状硅铝酸盐MAS-20的合成与表征 [J]. 高等学校化学学报 2011.
[6] 何红运, 李艳凤, 何震, 喻铃, 庞文琴, HE Hong-Yun, LI Yan-Feng, HE Zhen, YU Ling, PANG Wen-Qin. 全硅β沸石的合成、表征及在苯酚羟基化反应中的催化性能 [J]. 应用化学 2007.doi:10.3969/j.issn.1000-0518.2007.07.014
[7] 杨群保, 李永祥, 殷庆瑞, 王佩玲, 程一兵. 晶化时间对水热法制备钛酸铋纳米粉体的研究 [J]. 功能材料 2004.doi:10.3321/j.issn:1001-9731.2004.05.018
[8] Zekai Zhang, Shenglin liu, Xiangxue Zhu. Modification of Hbeta zeolite by fluorine and its influence on olefin alkylation thiophenic sulfur in gasoline [J]. Fuel Processing Technology 2008, 1(1).
[9] Bin Guo, Liangfang Zhu, Xiaoke Hu. Nature of vanadium species on vanadium silicalite-1 zeolite and their stability in hydroxylation reaction of benzene to phenol [J]. Catalysis science & technology 2011, 6(6).
[10] BAI Guoyi, DOU Haiyang, QIU Mande. Friedel-crafts hydroxyalkylation of anisole over oxalic acid modifed Hβ zeolite [J]. Catalysis Letters 2010, 138(3-4).
[11] Vivek Polshettiwar, Rajender S. Varina. Green chemistry by nano-catalysis [J]. Green chemistry 2010, 5(5).
[12] Beale AM., Sankar G.. In situ study of the formation of crystalline bismuth molybdate materials under hydrothermal conditions [J]. Chemistry of Materials 2003, 1(1).
[13] M.Karthik, A.K.Tripathi, N.M.Gupta, M.Palanichamy, V.Murugesan. Zeolite catalyzed electrophilic substitution reaction of indoles with aldehydes:synthesis of bis(indolyl)methanes [J]. Catalysis Communications 2004, 7(7).
