微波辐射固相合成外消旋1,1′-联-2-萘酚的改进

  • 马志广 ,
  • 郄录江 ,
  • 刘秀英 ,
  • 单金缓 ,
  • 申世刚
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  • 1.河北大学,化学与环境科学学院,河北,保定,071002; 2.河北大学 化学与环境科学学院, 河北 保定 071002

网络出版日期: 2001-10-25

A New Method for the Solid-phase Synthesis of Racemic 1,1′ -Bi-2-Naphthol Under Microwave Irradiation

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Online published: 2001-10-25

摘要

利用微波辐射,以FeCl3*6H2O为催化剂,使2-萘酚进行氧化偶联反应,合成外消旋1,1′-联-2-萘酚,反应时间2 min,产品产率98.5%,m.p.215~216 ℃.

本文引用格式

马志广 , 郄录江 , 刘秀英 , 单金缓 , 申世刚 . 微波辐射固相合成外消旋1,1′-联-2-萘酚的改进[J]. 河北大学学报(自然科学版), 2001 , 21(4) : 389 -390 . DOI: 10.3969/j.issn.1000-1565.2001.04.012

参考文献

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