微波辐射下快速合成乙酸酚酯

  • 李慧章 ,
  • 刘卉闵 ,
  • 肖立伟
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  • 1.河北大学,化学与环境科学学院,河北,保定,071002; 2.河北大学,化学与环境科学学院,河北,保定,071002;河北农业大学,理学院,河北,保定,071001

网络出版日期: 2003-08-25

基金资助

河北省自然科学基金

An Efficient Procedure for Acetylation of Phenols Under Microwave Irradiation

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Online published: 2003-08-25

摘要

在微波辐射下,研究了一系列的酚与乙酸酐的酰化反应,收率为75%~99%.此方法操作简便、反应收率高、时间短(10~180 s),是合成乙酸酚酯的简单易行的方法.

关键词: 乙酰化; 酚; 乙酸酐; 微波

本文引用格式

李慧章 , 刘卉闵 , 肖立伟 . 微波辐射下快速合成乙酸酚酯[J]. 河北大学学报(自然科学版), 2003 , 23(3) : 262 -264,301 . DOI: 10.3969/j.issn.1000-1565.2003.03.009

Abstract

The acetylation of phenols with acetic anhydride under microwave irradition was studied.The yield of the reaction is high(75%~95%) in short reaction time (10~180 s),providing a simple and efficient method to synthesize those compounds.

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