Synthesis of 5,6-Dihydro-2,3-Diphenyl-1,4-Dioxeneand 5,6-Dihydro-2,3-Diphenyl-1,4-Oxathiin under Microwave Irradiation

doi:10.3969/j.issn.1000-1565.2001.01.011

Abstract

CLC Number:

O621.3

LI Hui-zhang,YANG Xu-zhe,LI Tong-shuang,WANG Shu-xiang,LI Ji-tai. Synthesis of 5,6-Dihydro-2,3-Diphenyl-1,4-Dioxeneand 5,6-Dihydro-2,3-Diphenyl-1,4-Oxathiin under Microwave Irradiation[J]. Journal of Hebei University (Natural Science Edition), 2001, 21(1): 45-48.

References

[1] Loupy A., Hamelin J., Texier-Boullet F., Jacquault P., Mathe D., Petit A.. New solvent free organic synthesis using focused microwaves [Review] [J]. Synthesis: International Journal of Methods in Synthetic Organic Chemistry 1998, 9(9).
[2] 陆模文, 胡文祥, 恽榴红. 有机微波化学研究进展 [J]. 有机化学 1995, 15.
[3] 徐美忠, 谢毓元. 用微波炉加快有机化学反应速度 [J]. 化学通报(印刷版) 1993.
[4] 张力学, 丁金昌, 谷亨杰. 微波技术在有机合成中的应用 [J]. 1996.
[5] Bose A K, MANHAS M S, GHOSH M. Microwave-induced organic rea ction e nhancement chemistry 2:simplified techniques [J]. Journal of Organic Chemistry 1991, 56.
[6] Mojtahedi M M, SAIDI M R, BOLOURTCHIAN M. A novel method for the sy nthesis of disubstituted ureas and thioureas under microwave irradiation [J]. Journal of Chemical Research 1999.
[7] Hajipour A R, MALLAKPOUR S E, IMANZADEH G. A rapid and conve nient synthesis of oximes in dry media under microwave irradiation [J]. Journal of Chemical Research 1999.
[8] Harsha G. Jaisinghani, Bhushan M. Khadilkar. Microwave assisted, highly efficient solid state N- and S-alkylation [J]. Synthetic Communications 1999, 21(21).
[9] Mojtahedi M M, SAIDI M R, BOLOURTCHIAN M. Microwave-ass isted aminolysis of epoxides under solvent-free conditions catalyzed by montmorillonite clay [J]. Journal of Chemical Research 1999.
[10] MESHRAM H M, SUMITHRA G, REDDY G S. Microwave thermo lysis Ⅴ:a rapid and selective method for the cleavage of THP ethers, acetals a n d acetonides using clay supported ammonium nitrate clayan in dry media [J]. Synthetic Communications 1999, 29.
[11] Bandgar B P, SADAVARTE V S, SABU K R. Microwave activation in organic synth esis:natural Indian clay, EPICR EPZGR EPZ10R as novel heterogenous catalysis fo r rapid synthesis of nitriles from aldoximes in absence of solvent [J]. Synthetic Communications 1999, 29.
[12] Moghaddam F M, GHAFFARZADEH M, ABDI-OSKOUI S H. Tandem fries reaction-addit ion under microwave irradiation in dry media: one-pot synthesis of flavanones [J]. Journal of Chemical Research 1999.
[13] Yu H M, CHEN S T, Tseng M J. Microwave-assisted heter ogene ous Benzil-Benzilic acid rearrangement [J]. Journal of Chemical Research 1999.
[14] Bhushan M. Khadilkar, Virendra R. Madyar. Fries rearrangement at atmospheric pressure using microwave irradiation [J]. Synthetic Communications 1999, 7(7).
[15] CHAKRABORTY V, BORDOLOI M. Microwave-assisted oxidation of alcoho ls by pyridinium chlorochromate [J]. Journal of Chemical Research 1999.
[16] 李慧章, 李同双, 于涛. 微波辐射下苯偶姻的干法氧化反应 [J]. 有机化学 1998, 18.
[17] M. M. Heravi, D. Ajami, K. Tabar-Heydar. Oxidation of alcohols by silica gel-supported bis (trimethylsilyl) chromate under microwave irradiation without solvent [J]. Synthetic Communications 1999, 2(2).
[18] Mitra A K, DE A, KARCHAUDHURI N. Microwave-assisted syn theses of 1, 2-diketones [J]. Journal of Chemical Research 1999.
[19] Palombi L., Scettri A., Bonadies F.. MICROWAVE-ASSISTED OXIDATION OF SATURATED AND UNSATURATED ALCOHOLS WITH T-BUTYL HYDROPEROXIDE AND ZEOLITES [J]. Tetrahedron 1997, 46(46).
[20] MATTAY J, DITTMER C. Synthesis of 1, 4-oxathiins and 5, 6-dihyd ro-1, 4-oxathiins [J]. Journal of Organic Chemistry 1986, 51.
[21] Nevalainen V, VAINIOTALO P. Eletron impact induced fragme ntation of dihydro-1, 4-oxathiines [J]. Organic Mass Spectrometry 1986, 21.
[22] SUMMERBELL R K, BERGER D R. Rearrangement of α-halogenat ed ethers Ⅱ:the preparation and some reactions of 2, 3-diphenyl-p-dioxene [J]. Journal of the American Chemical Society 1959, 81.