LI Xiao-liu
,
FENG Jun-na
,
WANG Dong-yue
,
CHEN Hua
,
WAN Su-ying
,
CAO Ke-qiang
. Microwave Assisted Synthesis and Biological Study of 3,4-Dihydropyrimidin-2 (1H)-ones[J]. Journal of Hebei University(Natural Science Edition), 2009
, 29(5)
: 489
-494
.
DOI: 10.3969/j.issn.1000-1565.2009.05.011
[1] 许申鸿, XU Shenhong. Biginelli反应介绍 [J]. 大学化学 2004.doi:10.3969/j.issn.1000-8438.2004.05.008
[2] 路军, 马怀让, 李万华, LU Jun, MA Huai-Rang, LI Wan-Hu. 三氯化铁催化的一锅法合成3, 4-二氢嘧啶-2-酮 [J]. 有机化学 2000.doi:10.3321/j.issn:0253-2786.2000.05.037
[3] 路军, 王飞利, 白银娟, 李万华. NiCl2·6H2O催化的Biginelli反应--一锅法合成3, 4-二氢嘧啶-2-酮 [J]. 有机化学 2002.doi:10.3321/j.issn:0253-2786.2002.10.017
[4] 彭家建, 邓友全. 室温离子液体催化一锅法合成3, 4-二氢嘧啶-2-酮 [J]. 有机化学 2002.doi:10.3321/j.issn:0253-2786.2002.01.012
[5] 邵国强. 离子液体中微波促进的Biginelli缩合反应 [J]. 合成化学 2004.doi:10.3969/j.issn.1005-1511.2004.04.006
[6] 王彩凤, 姜恒, 宫红, 王敏, 王之昌, WANG, Cai-Feng, JIANG, Heng, GONG, Hong, WANG, Min, WANG, Zhi-Chang. 无机锌盐催化脂肪醛的Biginelli反应 [J]. 有机化学 2006.doi:10.3321/j.issn:0253-2786.2006.03.011
[7] 沙耀武, 王宇, 葛俊, 王欣. 微波促进的杂环化合物合成研究 [J]. 有机化学 2001.doi:10.3321/j.issn:0253-2786.2001.02.003
[8] KAPPE C O. 100 years of the Biginelli dihydropyrimidine synthesis [J]. Tetrahedron 1993, 49.
[9] K APPE C O, STADLER A. The Biginelli dihydropyrimidine synthesis [J]. Organic Reaction 2004, 63.
[10] Hu EH., Dolling UH., Sidler DR.. Unprecedented catalytic three component one-pot condensation reaction: An efficient synthesis of 5-alkoxycarbonyl-4-aryl-3, 4-dihydropyrimidin-2(1H)-ones [J]. The Journal of Organic Chemistry 1998, 10(10).
[11] BOSE D S, FATIMA L, MEREYALA H B. Green chemistry approaches to the synthesis of 5-alkoxycarbonyl-4-aryi-3, 4-dihydropyrimidine-2 (1 H)-ones by a three-component coupling of one-pot condensation reaction:comparson of ethanol, water and solvent-free conditions [J]. Journal of Organic Chemistry 2002, 68.
[12] KAPPE C O, FALSONE S F. Polyphosphate ester-mediated synthesis of dihydropyrimidines:improved conditions for the Biginell reaction [J]. Synlett:Accounts and Rapid Communications In Synthetic Organic Chemistry 1998.
[13] Jiajian Peng, Youquan Deng. Ionic liquids catalyzed Biginelli reaction under solvent-free conditions [J]. Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry 2001, 34(34).
[14] Bigi F., Frullanti B., Maggi R., Sartori G., Carloni S.. A revision of the Biginelli reaction under solid acid catalysis. Solvent-free synthesis of dihydropyrimidines over montmorillonite KSF [J]. Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry 1999, 17(17).
[15] LI Yuxia, BAO Weiliang. Microwave-assisted solventless Biginelli reaction catalyzed by montmorillonite clay-SmCl3 6 H2 O system [J]. CHINESE CHEMICAL LETTERS 2003, 14.
[16] COTTERILL I C, USYATINSKY A Y, ARNOLD J M. Microwave assisted combinatorial chemistry synthesis of substituted pyridines [J]. Tetrahedron Letters 1998, 39.
[17] Jean Jacques Vanden Eynde, Nancy Hecq, Olga Kataeva, C.Oliver Kappe. Microwave-mediated regioselective synthesis of novel pyrimido[1, 2-a]pyrimidines under solvent-free conditions [J]. Tetrahedron 2001, 9(9).
[18] Yadav JS., Reddy EJ., Ramalingam T., Reddy BVS.. Microwave-assisted efficient synthesis of dihydro pyrimidines: improved high yielding protocol for the Biginelli reaction [J]. Journal of Chemical Research. Synopses 2000, 7(7).
[19] STEFANI H A, GATTI P M. 3, 4-dihydropyrimide-2 (1 H)-ones:fast synthesis under microwave irradiation in solvent free conditions [J]. Synthetic Communications 2000, 12.
[20] YADAV J S, REDDY K B. Ultrasoun-aecelerated synthesis of 3, 4-dihydropyrimidin-2(1H)-ones with ceric ammonium nitrate [J]. Journal of the Chemical Society 2001.
[21] Li JT., Han JF., Yang JH., Li TS.. An efficient synthesis of 3, 4-dihydropyrimidin-2-ones catalyzed by NH2SO3H under ultrasound irradiation [J]. Ultrasonics sonochemistry 2003, 3(3).
[22] Wipf P., Cunningham A.. A SOLID PHASE PROTOCOL OF THE BIGINELLI DIHYDROPYRIMIDINE SYNTHESIS SUITABLE FOR COMBINATORIAL CHEMISTRY [J]. Tetrahedron Letters 1995, 43(43).
[23] FU Nanyan, YUAN Yaofeng, CAO Zhong. Indium(Ⅲ) bromide-catalyzed preparation of dihydropyrlmidinones;improved protocol conditions for the Biginelli reaction [J]. Tetrahedron 2002, 58.
[24] Ahmad Shaabani, Ayoob Bazgir, Fatemeh Teimouri. Ammonium chloride-catalyzed one-pot synthesis of 3, 4-dihydropyrimidin-2-(1H)-ones under solvent-free conditions [J]. Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry 2003, 4(4).
[25] REDDY K R, REDDY C V, MAHESH M. New environmentally friendly solvent free synthesis of dihydropyrimidinones catalysed by N-butyl-N, N-dimethyl-a -phenylethylammonium bromide [J]. Tetrahedron Letters 2003, 44.