Journal of Hebei University (Natural Science Edition) ›› 2016, Vol. 36 ›› Issue (2): 129-133.DOI: 10.3969/j.issn.1000-1565.2016.02.004

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Gradient strontium-brushite coatings of medical titanium alloy surface

LI Xinchang,YAN Yuting,FANG Qian,LIANG Yongqiang   

  1. College of Stomatology, North China University of Science and Technology, Tangshan 063000, China
  • Received:2015-11-10 Online:2016-03-25 Published:2016-03-25

Abstract: The concentration gradient of strontium-doped brushite coatings was prepared by two steps electrochemical depositions on the surface of medical titanium alloy(Ti-6Al-4V),which provided valuable theoretical reference for the clinical application and further experimental research of titanium(alloy)coating.The chemical compositions of coatings was analyzed by X-ray diffractometer(XRD),and the concentration of doped strontium was examed by X-ray fluorescence spectrometer(XRF).Field emission scanning electron microscopy(SEM)was used to examine the morphology of strontium-doped brushite coatings.The biocompatibility of strontium-doped brushite coatings was judged preliminarily by hemolysis rate that was tested by hemolysis test in vitro.The concentration of strontium was calculated according to the ratio of n(Sr)/n(Sr+Ga).Our results showed the concentrations of strontium-doped for strontium-doped brushite coatings were the percent of 10,15 and 20.The SEM images showed that the morphology of coatings was regular and compact.The rate of hemolysis was less than 5%,which was in accordance with the requirements of medical materials(<5%).

Key words: medical titanium alloy, electrochemical deposition, strontium, brushite, coating

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